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First direct insight into the local environment and dynamics of water molecules in the whewellite mineral phase: mechanochemical isotopic enrichment and high-resolution 17 O and 2 H NMR analyses

 Ieva Goldberga , Nicolas Patris , Chia-Hsin Chen , Emilie Thomassot , Julien Trébosc , et al.
2023
Pré-publication, Document de travail hal-04254127v1
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Amino Acids and Peptides in Ball Milling

 Thomas-Xavier Métro , Evelina Colacino , Jean Martinez , Frédéric Lamaty
Achim Stolle; Brindaban Ranu. Ball Milling Towards Green Synthesis: Applications, Projects, Challenges, Royal Society of Chemistry, pp.114-150, 2014, 978-1-78262-348-9. ⟨10.1039/9781782621980-00114⟩
Chapitre d'ouvrage istex hal-02364140v1
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Expedient Mechanosynthesis of N,N-Dialkyl Imidazoliums and Silver(I)-Carbene Complexes in a Ball-Mill

 Audrey Beillard , Ethan Golliard , Valentin Gillet , Xavier Bantreil , Thomas-Xavier Métro , et al.
Chemistry - A European Journal, 2015, 21 (49), pp.17614-17617. ⟨10.1002/chem.201503472⟩
Article dans une revue istex hal-02364136v1
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Solving the Challenging Synthesis of Highly Cytotoxic Silver Complexes bearing Sterically Hindered NHC Ligands with Mechanochemistry

 Audrey Beillard , François Quintin , Jérémie Gatignol , Pascal Retailleau , Jean-Luc Renaud , et al.
Dalton Transactions, 2020, 49 (36), pp.12592-12598. ⟨10.1039/D0DT00410C⟩
Article dans une revue hal-02919846v1
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Solvent-free synthesis of a formaldehyde-free benzoxazine monomer: study of its curing acceleration effect for commercial benzoxazine

 Romain Tavernier , Lérys Granado , Monique Tillard , Louis van Renterghem , Thomas-Xavier Métro , et al.
Polymer Chemistry, 2022, 13 (40), pp.5745-5756. ⟨10.1039/d2py00462c⟩
Article dans une revue hal-03819630v1
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Operando acoustic analysis: a valuable method for investigating reaction mechanisms in mechanochemistry

 César Leroy , Sébastien Mittelette , Gautier Félix , Nicolas Fabregue , Jessica Špačková , et al.
2023
Pré-publication, Document de travail hal-04259751v1
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Induction-heated ball-milling: a promising asset for mechanochemical reactions

 Gautier Félix , Nicolas Fabregue , César Leroy , Thomas-Xavier Métro , Chia-Hsin Chen , et al.
Physical Chemistry Chemical Physics, 2023, 25 (35), pp.23435-23447. ⟨10.1039/d3cp02540c⟩
Article dans une revue hal-04225761v3
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17O solid state NMR as a valuable tool for deciphering reaction mechanisms in mechanochemistry: the case study on the 17 O-enrichment of hydrated Ca-pyrophosphate biominerals

 Ieva Goldberga , Nicholai D Jensen , Christèle Combes , Frédéric Mentink-Vigier , Xiaoling Wang , et al.
Faraday Discussions, 2023, 241, pp.250-265. ⟨10.1039/d2fd00127f⟩
Article dans une revue hal-03846476v1
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A3-Coupling Reaction and [Ag(IPr)2]PF6: A Successful Couple

 Audrey Beillard , Thomas-Xavier Métro , Xavier Bantreil , Jean Martinez , Frédéric Lamaty
European Journal of Organic Chemistry, 2017, 2017 (31), pp.4642-4647. ⟨10.1002/ejoc.201700985⟩
Article dans une revue hal-02338923v1
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Gram‐Scale Synthesis of a Hexapeptide by Fragment Coupling in a Ball Mill

 Yves Yeboue , Nadia Rguioueg , Gilles Subra , Jean Martinez , Frédéric Lamaty , et al.
European Journal of Organic Chemistry, 2021, ⟨10.1002/ejoc.202100839⟩
Article dans une revue hal-03348943v1
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Peptide synthesis: ball-milling, in solution, or on solid support, what is the best strategy?

 Ophélie Maurin , Pascal Verdié , Gilles Subra , Frédéric Lamaty , Jean Martinez , et al.
Beilstein Journal of Organic Chemistry, 2017, 13, pp.2087-2093. ⟨10.3762/bjoc.13.206⟩
Article dans une revue hal-02336152v1
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Highly Enantioselective Synthesis of β-Amino Alcohols

 Thomas-Xavier Métro , Jérôme Appenzeller , Domingo Gomez Pardo , Janine Cossy
Organic Letters, 2006, 8, pp.3509 - 3512. ⟨10.1021/ol061133d⟩
Article dans une revue hal-03230701v1

Synthèse peptidique continue, sans solvant et non enzymatique par extrusion réactive

 Yves Yeboue , Benjamin Gallard , Nicolas Le Moigne , Frédéric Lamaty , Jean Martinez , et al.
France, Patent n° : EP3527580. 2018
Brevet hal-02503681v1
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Looking into the dynamics of molecular crystals of ibuprofen and terephthalic acid using 17O and 2H NMR analyses

 Chia‐hsin Chen , Ieva Goldberga , Philippe Gaveau , Sébastien Mittelette , Jessica Špačková , et al.
Magnetic Resonance in Chemistry, 2021, 59, pp.975. ⟨10.1002/mrc.5141⟩
Article dans une revue hal-03205685v1
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Sustainability and efficiency assessment of vanillin allylation: in solution versus ball-milling

 Damien Breilly , Sami Fadlallah , Vincent Froidevaux , Frédéric Lamaty , Florent Allais , et al.
Green Chemistry, 2022, 24, pp.7874-7882. ⟨10.1039/D2GC02185D⟩
Article dans une revue hal-03796375v1
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Cu(0), O2 and mechanical forces: a saving combination for efficient production of Cu-NHC complexes

 Audrey Beillard , Thomas-Xavier Métro , Xavier Bantreil , Jean Martinez , Frédéric Lamaty
Chemical Science, 2016, ⟨10.1039/c6sc03182j⟩
Article dans une revue hal-02336163v1

The Expanding Frontier Between Mechanochemistry & Solid State NMR: Special Focus on Inorganic Components of Materials

 César Leroy , Thomas-Xavier Métro , Danielle Laurencin
Reference Module in Chemistry, Molecular Sciences and Chemical Engineering, 2022, Elsevier, 2022, Reference Module in Chemistry, Molecular Sciences and Chemical Engineering, ⟨10.1016/B978-0-12-823144-9.00136-9⟩
Chapitre d'ouvrage hal-03841407v1
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From Operando Raman Mechanochemistry to “NMR Crystallography”: Understanding the Structures and Interconversion of Zn-Terephthalate Networks Using Selective 17 O-Labeling

 César Leroy , Thomas-Xavier Métro , Ivan Hung , Zhehong Gan , Christel Gervais , et al.
Chemistry of Materials, 2022, 34 (5), pp.2292-2312. ⟨10.1021/acs.chemmater.1c04132⟩
Article dans une revue hal-03681123v1
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Unraveling the synthesis of homoleptic [Ag(N,N-diaryl-NHC)2]Y (Y = BF4, PF6) complexes by ball-milling

 Audrey Beillard , Xavier Bantreil , Thomas-Xavier Métro , Jean Martinez , Frédéric Lamaty
Dalton Transactions, 2016, 45 (44), pp.17859-17866. ⟨10.1039/C6DT03564G⟩
Article dans une revue hal-02364127v1
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Cost-efficient and user-friendly 17O/ 18O labeling procedures of fatty acids using mechanochemistry

 Jessica Špačková , Charlyn Fabra , Guillaume Cazals , Marie Hubert-Roux , Isabelle Schmitz-Afonso , et al.
Chemical Communications, 2021, 57 (55), pp.6812-6815. ⟨10.1039/D1CC02165F⟩
Article dans une revue hal-03322217v1
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Direct 17O-isotopic labeling of oxides using mechanochemistry

 Chia-Hsin Chen , Emeline Gaillard , Frederic Mentink-Vigier , Kuizhi Chen , Zhehong Gan , et al.
Inorganic Chemistry, 2020, 59 (18), pp.13050-13066. ⟨10.1021/acs.inorgchem.0c00208⟩
Article dans une revue hal-02504692v1
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A more sustainable and efficient access to IMes·HCl and IPr·HCl by ball-milling

 Audrey Beillard , Xavier Bantreil , Thomas-Xavier Métro , Jean Martinez , Frédéric Lamaty
Green Chemistry, 2018, 20 (5), pp.964-968. ⟨10.1039/C7GC03539J⟩
Article dans une revue hal-02326212v1
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Mechanochemistry for facilitated access to N,N-diaryl NHC metal complexes

 Audrey Beillard , Xavier Bantreil , Thomas-Xavier Métro , Jean Martinez , Frédéric Lamaty
New Journal of Chemistry, 2017, 41 (3), pp.1057-1063. ⟨10.1039/C6NJ02895K⟩
Article dans une revue hal-02338978v1
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Efficient CO2 Sequestration by a Solid-Gas Reaction Enabled by Mechanochemistry: The Case of L-Lysine

 Abdal-Azim Al-Terkawi , Frédéric Lamaty , Thomas-Xavier Métro
2020
Pré-publication, Document de travail hal-03000893v1
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1,1′-Carbonyldiimidazole and Mechanochemistry: A Shining Green Combination

 Thomas-Xavier Métro , Jean Martinez , Frédéric Lamaty
ACS Sustainable Chemistry & Engineering, 2017, 5 (11), pp.9599-9602. ⟨10.1021/acssuschemeng.7b03260⟩
Article dans une revue hal-02336136v1
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Epimerization-Free C-Term Activation of Peptide Fragments by Ball Milling

 Yves Yeboue , Marion Jean , Gilles Subra , Jean Martinez , Frédéric Lamaty , et al.
Organic Letters, 2021, 23 (3), pp.631-635. ⟨10.1021/acs.orglett.0c03209⟩
Article dans une revue hal-03228800v1
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Epimerization-free C-term Activation of Peptide Fragments by Ball-Milling

 Yves Yeboue , Marion Jean , Gilles Subra , Jean Martinez , Frédéric Lamaty , et al.
2020
Pré-publication, Document de travail hal-03000765v1
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Operando acoustic analysis: a valuable method for investigating reaction mechanisms in mechanochemistry

 César Leroy , Sébastien Mittelette , Gautier Félix , Nicolas Fabregue , Jessica Špačková , et al.
Chemical Science, 2022, 13, pp.6328-6334. ⟨10.1039/d2sc01496c⟩
Article dans une revue hal-03679879v1
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Association of liquid-assisted grinding with aging accelerates the inherently slow slipping-on of a dibenzo-24-crown-8 over the N -hydroxysuccinimide ester of an ammonium-containing thread

 Benjamin Riss-Yaw , Thomas-Xavier Métro , Frédéric Lamaty , Frédéric Coutrot
RSC Advances, 2019, 9 (37), pp.21587-21590. ⟨10.1039/C9RA05045K⟩
Article dans une revue hal-02322306v1
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Peptide Mechanosynthesis by Direct Coupling of N -Protected α-Amino Acids with Amino Esters

 Vincent Porte , Marion Thioloy , Titouan Pigoux , Thomas-Xavier Métro , Jean Martinez , et al.
European Journal of Organic Chemistry, 2016, 2016 (21), pp.3505-3508. ⟨10.1002/ejoc.201600617⟩
Article dans une revue istex hal-02364118v1
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