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Primostrato Solid-State NMR Enhanced by Dynamic Nuclear Polarization: Pentacoordinated Al 3+ Ions Are Only Located at the Surface of Hydrated γ-Alumina

Daniel Lee , Nghia Tuan Tuan Duong , Olivier Lafon , Gaël de Paëpe
Journal of Physical Chemistry C, 2014, 118 (43), pp.25065-25076. ⟨10.1021/jp508009x⟩
Article dans une revue hal-02043253v1

Matrix-Free DNP-Enhanced NMR Spectroscopy of Liposomes Using a Lipid-Anchored Biradical

Carlos Fernandez-De-Alba , Hiroki Takahashi , Alexandre Richard , Yves Chenavier , Lionel Dubois , et al.
Chemistry - A European Journal, 2015, 21 (12), pp.4512-4517. ⟨10.1002/chem.201404588⟩
Article dans une revue istex hal-01592879v1
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Biomolecular and Biological Applications of Solid-State NMR with Dynamic Nuclear Polarization Enhancement

Wing Ying Chow , Gaël de Paëpe , Sabine Hediger
Chemical Reviews, 2022, 122 (10), pp.9795-9847. ⟨10.1021/acs.chemrev.1c01043⟩
Article dans une revue hal-03658826v1

Characterization of heteronuclear decoupling through proton spin dynamics in solid-state nuclear magnetic resonance spectroscopy

Gaël de Paëpe , Bénédicte Elena-Herrmann , Lyndon Emsley
Journal of Chemical Physics, 2004, 121 (7), pp.3165 - 3180. ⟨10.1063/1.1773155⟩
Article dans une revue hal-01907024v1
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Optimization of an absolute sensitivity in a glassy matrix during DNP-enhanced multidimensional solid-state NMR experiments

Hiroki Takahashi , Carlos Fernandez-De-Alba , Daniel Lee , Vincent Maurel , Serge Gambarelli , et al.
Journal of Magnetic Resonance, 2014, 239, pp.91-99. ⟨10.1016/j.jmr.2013.12.005⟩
Article dans une revue hal-02043248v1

Ultra-low temperature MAS-DNP

Daniel Lee , Eric Bouleau , Pierre Saint-Bonnet , Sabine Hediger , Gael de Paepe
Journal of Magnetic Resonance, 2016, 264, pp.116-124. ⟨10.1016/j.jmr.2015.12.010⟩
Article dans une revue cea-01849839v1
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Rapid Natural-Abundance 2D 13 C- 13 C Correlation Spectroscopy Using Dynamic Nuclear Polarization Enhanced Solid-State NMR and Matrix-Free Sample Preparation

Hiroki Takahashi , Daniel Lee , Lionel Dubois , Michel Bardet , Sabine Hediger , et al.
Angewandte Chemie, 2012, 124 (47), pp.11936-11939. ⟨10.1002/anie.201206102⟩
Article dans une revue istex hal-02043242v1
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Untangling the condensation network of organosiloxanes on nanoparticles using 2D $^{29}$Si– $^{29}$Si solid-state NMR enhanced by dynamic nuclear polarization

Daniel Lee , Guillaume Monin , Nghia Tuan Tuan Duong , Isabel Zamanillo Lopez , Michel Bardet , et al.
Journal of the American Chemical Society, 2014, 136 (39), pp.13781-13788. ⟨10.1021/ja506688m⟩
Article dans une revue hal-02043250v1
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Computationally Assisted Design of Polarizing Agents for Dynamic Nuclear Polarization Enhanced NMR: The AsymPol Family

Frederic Mentink-Vigier , Ildefonso Marin-Montesinos , Anil Jagtap , Thomas Halbritter , Johan van Tol , et al.
Journal of the American Chemical Society, 2018, 140 (35), pp.11013-11019. ⟨10.1021/jacs.8b04911⟩
Article dans une revue hal-02043262v1

Pushing NMR sensitivity limits using dynamic nuclear polarization with closed-loop cryogenic helium sample spinning

Eric Bouleau , Pierre Saint-Bonnet , Frederic Mentink-Vigier , H. Takahashi , Jean-François Jacquot , et al.
Chemical Science, 2015, 6 (12), pp.6806-6812. ⟨10.1039/c5sc02819a⟩
Article dans une revue hal-01587521v1
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Natural isotopic abundance $^{13}$C and $^{15}$N multidimensional solid-state NMR enabled by dynamic nuclear polarization

Adam Smith , Katharina Märker , Sabine Hediger , Gaël de Paëpe
Journal of Physical Chemistry Letters, 2019, 10 (16), pp.4652-4662. ⟨10.1021/acs.jpclett.8b03874⟩
Article dans une revue hal-02322267v1
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MAS-DNP Enhancements: Hyperpolarization, Depolarization, and Absolute Sensitivity

Sabine Hediger , Daniel Lee , Frederic Mentink-Vigier , Gaël de Paëpe
eMagRes, 2018, 7, pp.105-116. ⟨10.1002/9780470034590.emrstm1559⟩
Article dans une revue hal-02048719v1
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Selective high-resolution DNP-enhanced NMR of biomolecular binding sites

Ildefonso Marin-Montesinos , David Goyard , Emilie Gillon , Olivier Renaudet , Anne Imberty , et al.
Chemical Science, 2019, 10, pp.3366-3374. ⟨10.1039/c8sc05696j⟩
Article dans une revue hal-02052471v1
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Detection of the Surface of Crystalline Y2O3 Using Direct 89Y Dynamic Nuclear Polarization

Nick J Brownbill , Daniel Lee , Gaël de Paëpe , Frédéric Blanc
Journal of Physical Chemistry Letters, 2019, 10 (12), pp.3501 - 3508. ⟨10.1021/acs.jpclett.9b01185⟩
Article dans une revue hal-04500587v1
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PyrroTriPol: a semi-rigid trityl-nitroxide for high field dynamic nuclear polarization

Thomas Halbritter , Rania Harrabi , Subhradip Paul , Johan van Tol , Daniel Lee , et al.
Chemical Science, 2023, 14 (14), pp.3852-3864. ⟨10.1039/d2sc05880d⟩
Article dans une revue hal-04234725v1
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Sonocrystallization of CMONS Needles and Nanocubes: Mechanistic Studies and Advanced Crystallinity Characterization by Combining X-ray and Electron Diffractions with DNP-Enhanced NMR

X. Cattoen , Akshay Kumar , Carole Vaillant , Mauricio Matta-Seclén , Fabien Dubois , et al.
Crystal Growth & Design, 2022, 22 (4), pp.2181-2191. ⟨10.1021/acs.cgd.1c01246⟩
Article dans une revue hal-03619683v1

Nuclear depolarization and absolute sensitivity in magic-angle spinning cross effect dynamic nuclear polarization

Frederic Mentink-Vigier , Subhradip Paul , Daniel Lee , Akiva Feintuch , Sabine Hediger , et al.
Physical Chemistry Chemical Physics, 2015, 17 (34), pp.21824-21836. ⟨10.1039/c5cp03457d⟩
Article dans une revue cea-01734609v1

Dynamic Nuclear Polarization NMR of Low-γ Nuclei: Structural Insights into Hydrated Yttrium-Doped BaZrO 3

Frédéric Blanc , Luke Sperrin , Daniel Lee , Riza Dervişoğlu , Yoshihiro Yamazaki , et al.
Journal of Physical Chemistry Letters, 2014, 5 (14), pp.2431-2436
Article dans une revue hal-02043249v1

Transverse Dephasing Optimised NMR Spectroscopy in Solids: Natural-Abundance13C Correlation Spectra

Gaël de Paëpe , Anne Lesage , Stefan Steuernagel , Lyndon Emsley
ChemPhysChem, 2004, 5 (6), pp.869 - 875. ⟨10.1002/cphc.200301062⟩
Article dans une revue istex hal-01907029v1

ZnO Nanoplatelets with Controlled Thickness: Atomic Insight into Facet‐Specific Bimodal Ligand Binding Using DNP NMR

Michał Terlecki , Saumya Badoni , Michał Leszczyński , Stanisław Gierlotka , Iwona Justyniak , et al.
Advanced Functional Materials, 2021, pp.2105318. ⟨10.1002/adfm.202105318⟩
Article dans une revue hal-03356740v1
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Fast and accurate MAS–DNP simulations of large spin ensembles

Frederic Mentink-Vigier , Shimon Vega , Gaël de Paëpe
Physical Chemistry Chemical Physics, 2017, 19 (5), pp.3506-3522. ⟨10.1039/c6cp07881h⟩
Article dans une revue hal-02048457v1
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High-Field Solid-State NMR with Dynamic Nuclear Polarization

Daniel Lee , Sabine Hediger , Gaël De Paëpe
Modern Magnetic Resonance 2017, Springer International Publishing, pp.1-17, 2017, ⟨10.1007/978-3-319-28275-6_73-1⟩
Chapitre d'ouvrage hal-02043260v1
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Sparsely Pillared Graphene Materials for High-Performance Supercapacitors: Improving Ion Transport and Storage Capacity

Harish Banda , Sandy Périé , Barbara Daffos , Pierre-Louis Taberna , Lionel Dubois , et al.
ACS Nano, 2019, 13 (2), pp.1443-1453. ⟨10.1021/acsnano.8b07102⟩
Article dans une revue hal-02079872v1

Is solid-state NMR enhanced by dynamic nuclear polarization?

Daniel Lee , Sabine Hediger , Gael de Paepe
Solid State Nuclear Magnetic Resonance, 2015, 66-67, pp.6-20. ⟨10.1016/j.ssnmr.2015.01.003⟩
Article dans une revue cea-01731479v1
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Interfacial Ca2+ environments in nanocrystalline apatites revealed by dynamic nuclear polarization enhanced 43Ca NMR spectroscopy

Daniel Lee , César Leroy , Charlene Crevant , Laure Bonhomme-Coury , Florence Babonneau , et al.
Nature Communications, 2017, 8, pp.14104. ⟨10.1038/ncomms14104⟩
Article dans une revue hal-01448516v1

Solvent-derived defects suppress adsorption in MOF-74

Yao Fu , Yifeng Yao , Alexander Forse , Jianhua Li , Kenji Mochizuki , et al.
Nature Communications, 2023, 14 (1), pp.2386. ⟨10.1038/s41467-023-38155-8⟩
Article dans une revue hal-04500729v1
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The surface chemistry of a nanocellulose drug carrier unravelled by MAS-DNP

Akshay Kumar , Hippolyte Durand , Elisa Zeno , Cyril Balsollier , Bastien Watbled , et al.
Chemical Science, 2020, 11 (15), pp.3868-3877. ⟨10.1039/C9SC06312A⟩
Article dans une revue hal-02566887v1

On the use of radio‐frequency offsets for improving double‐quantum homonuclear dipolar recoupling of half‐integer‐spin quadrupolar nuclei

Nghia Tuan Duong , Daniel Lee , Frédéric Mentink‐vigier , Olivier Lafon , Gaël de Paëpe
Magnetic Resonance in Chemistry, 2021, 59 (9-10), pp.991-1008. ⟨10.1002/mrc.5142⟩
Article dans une revue hal-03356733v1
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Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

Katharina Märker , Sabine Hediger , Gaël de Paëpe
Chemical Communications, 2017, 53 (65), pp.9155-9158. ⟨10.1039/C7CC04890D⟩
Article dans une revue hal-02048398v1
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Welcoming natural isotopic abundance in solid-state NMR: probing π-stacking and supramolecular structure of organic nanoassemblies using DNP

Katharina Märker , Subhradip Paul , Carlos Fernandez-De-Alba , Daniel Lee , Jean-Marie Mouesca , et al.
Chemical Science, 2017, 8 (2), pp.974-987. ⟨10.1039/c6sc02709a⟩
Article dans une revue hal-02072153v1